3-Benzyl­sulfanyl-1H-1,2,4-triazol-5-amine

نویسندگان

  • Shuai Zhang
  • Pei-Jiang Liu
  • Dong-Sheng Ma
  • Guang-Feng Hou
چکیده

In the title mol-ecule, C(9)H(10)N(4)S, the dihedral angle between the benzene and triazole rings is 81.05 (5)°. In the crystal, N-H⋯N hydrogen bonds link the mol-ecules into infinite zigzag chains along [010].

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منابع مشابه

3-Benzyl­sulfanyl-5-(4-phenyl-1H-1,2,3-triazol-1-ylmeth­yl)-4H-1,2,4-triazol-4-amine

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3-Phenyl-1H-1,2,4-triazol-5-amine–5-phenyl-1H-1,2,4-triazol-3-amine (1/1)

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N-[(Z)-(1-Methyl-1H-pyrrol-2-yl)methyl­idene]-1H-1,2,4-triazol-5-amine

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N-[(E)-(5-Methyl­thio­phen-2-yl)methyl­idene]-1H-1,2,4-triazol-3-amine

In the title Schiff base, C(8)H(8)N(4)S, a condensation product of 5-methyl-thio-phene-2-carboxaldehyde and 3-amino-1,2,4-triazole, the dihedral angle between the triazolyl and thienyl rings is 6.44 (14)°. The compound exists as a polymeric chain arising from inter-molecular N-H⋯N bonding.

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Synthesis and determination of pKa values of some new 3,4-disubstituted-4,5-dihydro-1H-1,2,4-triazol-5-one derivatives in non-aqueous solvents.

3-Alkyl(Aryl)-4-amino-4,5-dihydro-1H-1,2,4-triazol-5-ones (2) reacted with 2-furoyl chloride and thiophene-2-carbonyl chloride to afford the corresponding 3- alkyl(aryl)-4-(2-furoylamino)-4,5-dihydro-1H-1,2,4-triazol-5-ones (3) and 3-alkyl(aryl)- 4-(2-thienylcarbonylamino)-4,5-dihydro-1H-1,2,4-triazol-5-ones (4), respectively. The new compounds synthesized were characterized by using IR, 1H-NMR...

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عنوان ژورنال:

دوره 68  شماره 

صفحات  -

تاریخ انتشار 2012